Experimental Methods in Organic Chemistry

 

 

James A. Moore and David L. Dalrympler

Hardcover: 334 pagina's 

Uitgever: W.B. Saunders; (1976); 2nd ed.; ISBN 072166521

 

Contents

  • Introduction
  • Crystallization
  • Extraction
  • Distillation
  • Vapor phase chromatography
  • Liquid phase chromatography
  • Steam distillation of essential oils
  • Infrared absorption spectroscopy
  • Nuclear magnetic resonance spectroscopy
  • The literature of organic chemistry
  • Free radical chlorination
  • The Diels-Alder reaction
  • Nucleophilic substitution of alkyl halides
  • Dehydration of alcohols
  • Preparation of cyclohexyl chloride
  • The Grignard reaction
  • Preparation and stereochemistry of bicyclic alcohols
  • Chromic acid oxidation  
  • Equilibrium constant for esterification
  • Effects of subsitituents on acidity
  • Effects of subsitituents on reactivity
  • Alkylation of the aromatic ring
  • Aromatic nitration
  • Aromatic nucleophilic substititution
  • Chemiluminescence
  • Photochemical reactions
  • Preparation of benzoic anhydride
  • The aldol condensation
  • Synthesis of a citrus bioregulator
  • Benzyne
  • Synthesis of Lidocaine
  • Heterocyclic syntheses
  • Synthesis of sulfa drugs
  • Resolution of alpha-phenylethylamine
  • Enzymatic resolution of DL-methionine
  • Chemistry of sugars
  • Hydrolysis of Starch
  • Kinetics of enzymatic and acid-catalyzed reactions
  • Analysis of fats and oils
  • Synthetic organic polymers
  • Dyes and dyeing
  • Identification of unknowns

23-12-2002